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A crystalline Sm(Ⅲ)-containing antimonotungstate with efficient catalytic activity in three-component reaction for isoindolinones synthesis 认领 引用 被引量：1
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作者 Hao-Qi Liu Jia-Wei Cao +6 位作者 Wei Tang Zhou-Fu Lin Ke Li Wei-Jian Xu Zhi-Bin Zhang Yu-Feng Liu Guo-Ping Yang 《Rare Metals》 SCIE EI CAS CSCD 2025年第6期3995-4002,共8页
The development of the three-component catalytic system for constructing isoindolinones from simple feedstocks is both significant and challenging.In this study,a unique tartrate-linked dimeric samarium-antimonotungst... The development of the three-component catalytic system for constructing isoindolinones from simple feedstocks is both significant and challenging.In this study,a unique tartrate-linked dimeric samarium-antimonotungstate[Sm2(H2O)6(tar)(Sb2W21O72)]220-(Sm4tar2,H4tar=tartaric acid)was synthesized via a one-step method at room temperature using an acetate buffer solution.The dimeric polyanion of Sm4tar2shows a centrosymmetric structure with a parallelogram-like arrangement and comprises two enantiomeric{Sm2(H2O)6(Sb2W21O72)}moieties connected by two enantiomeric tar ligands.Sm4tar2demonstrates efficient catalytic activity in the three-component reaction involving 2-acylbenzoic acids,primary amines,and phosphine oxides to form 3,3-disubstituted isoindolinones.The advantages of this catalytic system include simple feedstocks,green and reusable catalyst,and operational simplicity with water as the sole by-product.This finding enables an effective molecular fragment assembly strategy for synthesizing isoindolinone drug precursor skeletons. 展开更多
关键词 Samarium Antimonotungstate Tartaric acid Three-component reaction Isoindolinones
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Photocatalyst-free visible-light-mediated three-component reaction ofα-diazoesters, cyclic ethers and NaSCN to access organic thiocyanates 认领 引用 被引量：4
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作者 Zhiwei Wang Na Meng +3 位作者 Yufen Lv Wei Wei Huilan Yue Guofu Zhong 《Chinese Chemical Letters》 SCIE CAS CSCD 2023年第2期198-201,共4页
A facile and environmentally friendly visible-light-induced three-component reaction of α-diazoesters,cyclic ethers and Na SCN to construct organic thiocyanates has been developed at room temperature. This reaction c... A facile and environmentally friendly visible-light-induced three-component reaction of α-diazoesters,cyclic ethers and Na SCN to construct organic thiocyanates has been developed at room temperature. This reaction could occur under photocatalyst-and additive-free conditions to afford a number of organic thiocyanates with moderate to good yield and favorable functional group tolerance. 展开更多
关键词 Photocatalyst-free Visible-light Three-component reaction Organic thiocyanates
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Visible-light-induced three-component reaction of quinoxalin-2(1H)-ones,alkenes and CF3SO2Na leading to 3-trifluoroalkylated quinoxalin-2(1H)-ones 认领 引用 被引量：4
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作者 Na Menga Yufen Lv +3 位作者 Qishun Liu Ruisheng Liu Xiaohui Zhao Wei Wei 《Chinese Chemical Letters》 SCIE CAS CSCD 2021年第1期258-262,共5页
A facile and metal-free visible-light-enabled three-component reaction of quinoxalin-2(1 H)-ones,alkenes and CF3SO2Na has been developed under air at room temperature.This photocatalytic tandem reaction using 4 ... A facile and metal-free visible-light-enabled three-component reaction of quinoxalin-2(1 H)-ones,alkenes and CF3SO2Na has been developed under air at room temperature.This photocatalytic tandem reaction using 4 CzIPN as the photocatalyst and air as the green oxidant,provides a mild and environmentally friendly approach to access a series of 3-trifluoroalkylated quinoxalin-2(1 H)-ones. 展开更多
关键词 Metal-free Visible-light-catalysis Three-component reaction Quinoxalin-2(1H)-ones
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Three-component reaction for synthesis of functionalized spiro[indoline-3,4'-pyrano[3,2-h]quinolines] 认领 引用 被引量：2
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作者 Rong-Guo Shi Chao-Guo Yan 《Chinese Chemical Letters》 SCIE CAS CSCD 2016年第4期575-578,共4页
The functionalized spiro[indoline-3,40-pyrano[3,2-h]quinolines] were efficiently prepared in high yields from three-component reaction of 8-hydroxyquinoline, isatins and malononitrile or ethyl cyanoacetate in ethanol ... The functionalized spiro[indoline-3,40-pyrano[3,2-h]quinolines] were efficiently prepared in high yields from three-component reaction of 8-hydroxyquinoline, isatins and malononitrile or ethyl cyanoacetate in ethanol at room temperature for about 12 h in the presence of piperidine. 展开更多
关键词 Spirooxindole Chromene Isatin Malononitrile Three-component reaction
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A novel and green synthesis of indolone-N-amino acid derivatives via the Passerini three-component reactions in water 认领 引用 被引量：2
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作者 Rong-Kun Li Quan-Li Yang +3 位作者 Yi Liu Dong-Wei Li Nian-Yu Huang Ming-Guo Liu 《Chinese Chemical Letters》 SCIE CAS CSCD 2016年第3期345-348,共4页
A green Passerini three-component reaction of 2-（4-oxo-4,5,6,7-tetrahydro-1H-indol-1-yl）acetic acid with alkyl or aryl isocyanides and aldehydes was reported under aqueous conditions at 35 ℃ for 1 h, and21 indolone... A green Passerini three-component reaction of 2-（4-oxo-4,5,6,7-tetrahydro-1H-indol-1-yl）acetic acid with alkyl or aryl isocyanides and aldehydes was reported under aqueous conditions at 35 ℃ for 1 h, and21 indolone-N-amino acid derivatives were prepared in high yields of 42%–99%. Their structures were characterized by IR, ESI–MS, NMR and elemental analysis, and the possible mechanisms have been also proposed. The highly efficient and eco-friendly method provides a facile access to a library of indoloneN-amino acid derivatives for future research on bioactivity screening. 展开更多
关键词 Passerini three-component reaction Indolone-N-amino acid Green synthesis Heterocycles Isocyanide
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A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide 认领 引用 被引量：1
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作者 Barahman Movassagh Amir Rakhshani 《Chinese Chemical Letters》 SCIE CAS CSCD 2011年第10期1179-1182,共4页
Potassium tert-butoxide has been found to be a highly efficient catalyst for one-pot,three-component reaction of aryl aldehydes, acetophenones,and thiols via Claisen-Schmidt/Michael addition reactions for the synthesi... Potassium tert-butoxide has been found to be a highly efficient catalyst for one-pot,three-component reaction of aryl aldehydes, acetophenones,and thiols via Claisen-Schmidt/Michael addition reactions for the synthesis of thia-Michael adducts in high yields. The reactions are best carried out in tert-butyl alcohol at room temperature. 展开更多
关键词 Potassium tert-butoxide Thia-Michael adduct Three-component reaction C-S bond formation Thiols
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Facile synthesis of N-(arylsulfonyl)-4-ethoxy-5-oxo-2,5-dihydro-1H-pyrolle-2,3-dicarboxylates by one-pot three-component reaction 认领 引用 被引量：4
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作者 Hossein Anaraki-Ardakani Maziar Noei Afrooz Tabarzad 《Chinese Chemical Letters》 SCIE CAS CSCD 2012年第1期45-48,共4页
Three-component reaction of arylsulfonamides,dialkyl acetylenedicarboxylates,and ethyl chlorooxoacetate promoted by triphenylphosphine and triethylamine provides a sufficient route for the synthesis of dialkyl N-（ary... Three-component reaction of arylsulfonamides,dialkyl acetylenedicarboxylates,and ethyl chlorooxoacetate promoted by triphenylphosphine and triethylamine provides a sufficient route for the synthesis of dialkyl N-（arylsulfonyl）-4-ethoxy-5-oxo-2,5-dihydro -1H-pyrolle-2,3-dicarboxylates in good yields. 展开更多
关键词 Arylsulfonamides Dialkyl acetylenedicarboxylates Triphenylphosphine Multi-component reactions 3-Pyrollin-2-ones
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Efficient approach to thiazolidinones via a one-pot three-component reaction involving 2-amino-1-phenylethanone hydrochloride,aldehyde and mercaptoacetic acid 认领 引用 被引量：1
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作者 Asha Vasantrao Chate Akash Gitaram Tathe +2 位作者 Prajyot Jayadev Nagtilak Sunil M.Sangle Charansingh H.Gill 《Chinese Journal of Catalysis》 SCIE EI CAS CSCD 北大核心 2016年第11期1997-2002,共6页
A highly efficient three-component reaction has been developed for the synthesis of thiazolidinones involving the reaction of 2-amino-l-phenylethanone hydrochloride with an aromatic aldehyde and mercaptoacetic acid in... A highly efficient three-component reaction has been developed for the synthesis of thiazolidinones involving the reaction of 2-amino-l-phenylethanone hydrochloride with an aromatic aldehyde and mercaptoacetic acid in the presence of diisopropylethylamine in a single pot.Critically,this reaction exhibited excellent chemoselectivity,with the nitrogen atom of the 2-amino-l-phenylethanone component reacting selectively with the aromatic aldehyde to give the corresponding Schiff base.Nucleophilic attack at the carbon of the Schiff base by the sulfur atom of mercaptoacetic,followed by a cyclocondensation reaction between the nitrogen and the carboxylic acid moiety afforded the desired thiazolidinones,which were fully characterized by spectroscopic techniques. 展开更多
关键词 Tandem reaction Thiazolidinones Heterocycles N N-diisopropylethylamine Cyclization
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Silver-catalyzed three-component reaction of phenyldiazoacetate with arylamine and imine 认领 引用
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作者 Bai‐Ling Chen Zhen Wang +2 位作者 You‐Can Zhang Zhi‐Gang Zhao Zili Chen 《Chinese Journal of Catalysis》 SCIE EI CAS CSCD 北大核心 2018年第10期1594-1598,共5页
A new method was developed to diastereoselectively synthesize polysubstituted 1,2‐diamine compounds from the reaction of diazoesters with arylamines and diaryl imines by using the dioxazoline ligand L2‐ligated silve... A new method was developed to diastereoselectively synthesize polysubstituted 1,2‐diamine compounds from the reaction of diazoesters with arylamines and diaryl imines by using the dioxazoline ligand L2‐ligated silver catalyst.The Lewis acidity of the silver catalyst affected the different types of substrate diastereoselectivities;It also led to the formation of amine‐exchange side products. 展开更多
关键词 Silver catalysis Carbene transfer reaction Three‐component reaction Ammonium ylide Diamine compouds
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Metal-free one-pot synthesis of quinoline-2,4-carboxylates via a molecular iodine-catalyzed three-component reaction of arylamines, ethyl glyoxylate, and α-ketoesters 认领 引用 被引量：2
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作者 Guang-Ming Nan Wei Liu 《Chinese Chemical Letters》 SCIE CAS CSCD 2015年第10期1289-1292,共4页
A simple and metal-free method has been developed for the construction of quinoline-2,4-carboxylates under mild conditions via a molecular iodine-catalyzed three-component tandem reaction of arylamines, ethyl glyoxyla... A simple and metal-free method has been developed for the construction of quinoline-2,4-carboxylates under mild conditions via a molecular iodine-catalyzed three-component tandem reaction of arylamines, ethyl glyoxylate, and a-ketoesters. The present protocol provides a convenient and attractive approach to various quinoline-2,4-carboxylates in moderate to good yields with excellent functional group tolerance. 展开更多
关键词 Molecular iodine Quinoline-2 4-carboxylates Three-component Tandem reaction
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Synthesis of polysubstituted pyrroles via a gold(Ⅰ)-catalyzed tandem three-component reaction at room temperature 认领 引用 被引量：1
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作者 Li Li Qi Chen +5 位作者 Xiaonan Xiong Chuang Zhang Jingjing Qian Jie Shi Qiong An Ming Zhang 《Chinese Chemical Letters》 SCIE CAS CSCD 2018年第12期1893-1896,共4页
A gold(Ⅰ)-catalyzed three-component reaction of β-nitrostyrenes with 1,3-dicarbonyl compounds and primary amines to form polysubstituted pyrroles has been developed at room temperature in ethanol.The key advantages ... A gold(Ⅰ)-catalyzed three-component reaction of β-nitrostyrenes with 1,3-dicarbonyl compounds and primary amines to form polysubstituted pyrroles has been developed at room temperature in ethanol.The key advantages of the three-component reaction are the mild reaction conditions and environmentally safer solvent. 展开更多
关键词 Gold(I) complex Multicomponent reaction Nitrogen heterocycles Room temperature Pyrroles
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Electrochemical difunctionalization of isocyanides by a three-component reaction cascade Mumm rearrangement:Rapid access to sulfur-containing imides 认领 引用
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作者 Hongmei Jiang Zhibin Nong +6 位作者 Xi Chen Tiancheng Cai Hanxuan Zhang Rui Li Qiang Li Lei Liu Qing-Wen Gui 《Green Synthesis and Catalysis》 CSCD 2026年第1期119-123,共5页
An efficient and practical electrochemical method for the three-component reaction cascade Mumm rearrangement of imides has been developed using a simple undivided cell with carbon electrodes at room temperature,which... An efficient and practical electrochemical method for the three-component reaction cascade Mumm rearrangement of imides has been developed using a simple undivided cell with carbon electrodes at room temperature,which provides a useful strategy for the rapid synthesis of sulfur-containing imides with broad substrate scope and high functional tolerance.It is a rare example of in situ generation of O-acyl isoamide precursor for Mumm rearrangement. 展开更多
关键词 Electrochemical difunctionalization Cascade Mumm rearrangement Three-component reaction Sulfur-containing imides O-acyl isoamide
Three-component reaction of triphenylphosphine,dialkyl but-2-ynedioate and arylidene pivaloylacetonitrile for diastereoselective synthesis of densely substituted 2,3-dihydrofurans 认领 引用 被引量：1
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作者 Wen-Jie Qi Ying Han +1 位作者 Chang-Zhou Liu Chao-Guo Yan 《Chinese Chemical Letters》 SCIE CAS CSCD 2017年第2期442-445,共4页
The three-component reaction of triphenylphosphine,dialkyl but-2-ynedioate and arylidene pivaloylacetonitrile in dry methylene dichloride at room temperature resulted in unexpected densely substituted 1-（triphenyl-λ... The three-component reaction of triphenylphosphine,dialkyl but-2-ynedioate and arylidene pivaloylacetonitrile in dry methylene dichloride at room temperature resulted in unexpected densely substituted 1-（triphenyl-λ^5-phosphanylidene）ethyl）-2,3-dihydrofurans in satisfactory yields with high diastereoselectivity.The relative configuration of the 2,3-dihydrofurans was elucidated by determination of single crystal structures. 展开更多
关键词 Multicomponent reaction Triphenylphosphine But-2-ynedioate Pivaloylacetonitrile 2 3-Dihydrofuran
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Copper-catalyzed three-component reaction of imidazo[1,2-a]pyridine with elemental sulfur and arylboronic acid to produce sulfenylimidazo[1,2-a]pyridines 认领 引用
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作者 Genhua Xiao Hao Min +2 位作者 Zhilei Zheng Guobo Deng Yun Liang 《Chinese Chemical Letters》 SCIE CAS CSCD 2018年第9期1363-1366,共4页
In this work, an efficient copper-catalyzed three-component reaction for the synthesis of sulfenylimidazo [1,2-a]pyridines using elemental sulfur as the sulfenylating agents has been developed. The reaction could proc... In this work, an efficient copper-catalyzed three-component reaction for the synthesis of sulfenylimidazo [1,2-a]pyridines using elemental sulfur as the sulfenylating agents has been developed. The reaction could proceed smoothly with a high degree of functional group tolerance and provide the desired products in moderate to good yield. 展开更多
关键词 Copper Three-component Pyridine Sulfur Arylboronic acids
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Three-component Reaction of Aromatic Aldehyde,Malononitrile and Aliphatic Amine Leading to Different Pyridine Derivatives 认领 引用
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作者 CHEN Jiao MA Zhen YAN Chao-guo 《Chemical Research in Chinese Universities》 SCIE CAS 2010年第6期937-941,共5页
The three-component reaction of aromatic aldehyde,malononitrile and aliphatic amine in a mixed solvent of methanol and water exhibited very interesting molecular diversity and gave the derivatives of polysubstituted N... The three-component reaction of aromatic aldehyde,malononitrile and aliphatic amine in a mixed solvent of methanol and water exhibited very interesting molecular diversity and gave the derivatives of polysubstituted N-methyldihydropyridines,2-dialkylaminopyridines and 2-methoxypyridines as main products according to the structure of aliphatic amines used. 展开更多
关键词 Multicomponent reaction Malononitrile Aldehyde Dihydropyridine Pyridine Aminopyridine
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Identification of underwater suction vortex at the inlet of a ship's waterjet propulsion pump device via volumetric three-component velocimetry(V3V) 认领 引用
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作者 Weixuan Jiao Xuanwen Jia +1 位作者 Li Cheng Bowen Zhang 《Defence Technology（防务技术）》 SCIE EI CAS CSCD 2026年第6期254-272,共19页
Waterjet propulsion systems,as the predominant form of propulsion for high-performance vessels,are widely employed in military ships across various navies.However,when operating in shallow water conditions,underwater ... Waterjet propulsion systems,as the predominant form of propulsion for high-performance vessels,are widely employed in military ships across various navies.However,when operating in shallow water conditions,underwater suction vortices(USVs)are prone to form near the pump inlet.These vortices can markedly degrade the hydraulic performance of the waterjet propulsion system by reducing efficiency and potentially inducing cavitation and associated vibrations.The formation and evolution of USVs occur underwater,rendering them highly elusive and difficult to detect or measure accurately.As a result,investigating the underlying mechanisms of USV generation and developing effective control strategies remain substantial challenges in the field.To achieve precise identification and capture of USVs,volumetric three component velocimetry technology was employed to conduct high-precision analyses of the three-dimensional spatiotemporal evolution signals and vortex dynamic characteristics of USVs throughout their entire lifecycle.The findings demonstrate that the typical evolution of USVs can be categorized into five stages:precursor,inception,development,weakening,and dissipation.During their evolution,both velocity and vorticity within USVs initially increase before subsequently decreasing.Notably,the velocity distribution within the vortex core conforms to the Rankine composite vortex model.The adverse pressure gradient at the riverbed,combined with the suction flow of the pump,directly facilitates USV generation.These findings provide a critical foundation for USV identification,offering a valuable method for flow-field testing in vortex and other fault identification,while overcoming the limitations of conventional point sensors in complex flow diagnostics. 展开更多
关键词 Waterjet propulsion Vortex dynamics Spatiotemporal evolution Underwater suction vortex Volumetric three-component velocimetry Model test
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Efficient Synthesis of Pyrrolo[2,1-a]isoquinoline and Pyrrolo[1,2-a]quinoline Derivatives via One-pot Two- step Metal-catalyzed Three-component Reactions 认领 引用 被引量：2
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作者 吴磊 孙晶 颜朝国 《Chinese Journal of Chemistry》 SCIE CAS CSCD 2012年第3期590-596,共7页
A sequential one-pot two-step reaction for efficient synthesis of pyrrolo[2,1-a]isoquinoline and pyrrolo[1,2-a]- quinoline derivatives in good yields has been successfully developed. The reaction included firstly Cu-c... A sequential one-pot two-step reaction for efficient synthesis of pyrrolo[2,1-a]isoquinoline and pyrrolo[1,2-a]- quinoline derivatives in good yields has been successfully developed. The reaction included firstly Cu-catalyzed three-component reaction of isoquinoline （quinoline）, acetylenedicarboxylate and alkynylbenzene and then Pd-catalyzed intramolecular C（sp）-C（sp^2） coupling reaction of initially formed 1-alkenyl-2-alkynyl- 1,2-dihydroiso- quinoline （1,2-dihydroquinoline）. 展开更多
关键词 indolizine pyrrolo[2,1-a]isoquinoline isoquinoline C-C coupling reaction three-component reaction
Synthesis of benzisothiazoles by a three-component reaction using elemental sulfur and ammonium as heteroatom components under transition metal-free conditions 认领 引用 被引量：2
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作者 Min Wang Xia Meng +2 位作者 Changqun Cai Lingyun Wang Hang Gong 《Green Synthesis and Catalysis》 2022年第2期168-174,共7页
A strategy for the synthesis of benzisothiazoles by a three-component reaction was developed using elemental sulfur and ammonium as heteroatom components under transition metal-free conditions.The reaction is preferab... A strategy for the synthesis of benzisothiazoles by a three-component reaction was developed using elemental sulfur and ammonium as heteroatom components under transition metal-free conditions.The reaction is preferably based on pyridine or quinoline ring substrate,and good to excellent yields can be obtained.Notably,this reaction has been applied to the gram-scale synthesis of bioactive molecules. 展开更多
关键词 Synthetic methodology Three-component reaction Transition-metal free Sulfur Benzisothiazole
A H4SiW12O40-catalyzed three-component tandem reaction for the synthesis of 3,3-disubstituted isoindolinones 认领 引用 被引量：5
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作者 Yufeng Liu Guodong Zeng +4 位作者 Yutao Cheng Lei Chen Yunhai Liu Yongge Wei Guoping Yang 《Chinese Chemical Letters》 SCIE CAS CSCD 2024年第1期233-236,共4页
A H4SiW12O40-catalyzed three-component tandem reaction of 2-acylbenzoic acids,primary amines and phosphine oxides to form 3,3-disubstituted isoindolinones was developed.By employing A H4SiW12O40as th... A H4SiW12O40-catalyzed three-component tandem reaction of 2-acylbenzoic acids,primary amines and phosphine oxides to form 3,3-disubstituted isoindolinones was developed.By employing A H4SiW12O40as the catalyst and dimethyl carbonate(DMC)as the solvent,a diverse range of 2-acylbenzoic acid derivatives and primary amines worked well to give the C3-phosphinoyl-functionalized 3,3-disubstituted isoindolinones with the yield range of 61%-87%.Advantages of this transformation include green catalyst and solvent,available starting materials,broad substrate scope,high efficiency and operational simplicity with water as the sole by-product.The strategy achieved an efficient and green molecular fragment assembly to access isoindolinones,which would provide opportunities for the synthesis of potential biologically active molecules in a green manner. 展开更多
关键词 Polyoxometalates Dehydrative coupling Three-component tandem reaction 3,3-Disubstituted isoindolinones Organic carbonate
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Efficient and regioselective C=S bond difunctionalization through a three-component radical relay strategy 认领 引用 被引量：1
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作者 Shan-Shan Li Juan Luo +4 位作者 Shu-Nuo Liang Dan-Na Chen Li-Ning Chen Cheng-Xue Pan Peng-Ju Xia 《Chinese Chemical Letters》 SCIE CAS CSCD 2025年第6期455-461,共7页
A novel photocatalytic energy transfer-driven radical relay strategy has been introduced for the chemoand regioselective 1,4-difunctionalization of carbon-sulfur double bonds.This represents the first instance of radi... A novel photocatalytic energy transfer-driven radical relay strategy has been introduced for the chemoand regioselective 1,4-difunctionalization of carbon-sulfur double bonds.This represents the first instance of radical-mediated dual-functionalization of X-Y type unsaturated bonds,enabling the synthesis of complex linear molecules with C–O,C–N,and C-S bonds in a single operation.The method surpasses traditional approaches by avoiding the need for thiourea intermediates and the harsh conditions typically associated with them.The developed strategy exemplifies versatility,being applicable to 1,4-oxyamination,1,4-diamination,and 1,4-sulfonamination reactions,and has demonstrated compatibility with over 60 different substrates.The research also elucidates the role of electronic complementarity between radicals and receptors in achieving high selectivity in 1,4-difunctionalization reactions.This study significantly advances the field of bifunctionalization and remote difunctionalization reactions,with profound implications for the development of pharmaceuticals and materials science. 展开更多
关键词 Radical relay Selective 1,4-difunctionalization Multicomponent reactions Isothiocyanates C=S bonds
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